めっきの添加剤として用いられる水溶性高分子と界面活性剤を対象として、AFM、QCM-D、エリプソメトリーを用いて添加剤の電極表面への吸着状態とめっき反応抑制効果の関係を解析した。その結果、迅速に吸着しリジッドな膜を形成するCTABが最も高い電析抑制作用を示し、含水量が多くソフトな膜を形成するPVAは抑制効果が弱く、吸着速度が遅いLASでは抑制効果が非常に弱かった。液中AFMを用いてモルフォロジーの観察を行いこれらの結果を補強した。複数の解析手法を併用することで固液界面に存在するめっき添加剤の存在形態に関する情報を得ることができた。
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